Identifikasi Komponen Kimia Ekstrak Daun Ketapang (Terminalia cattapa) Berdasarkan Perbandingan Metode Ekstraksi

Abstract

Screening, characterization and identification of chemical components of typical Indonesian plants are important for the purpose of finding high potential chemical components in the use of primary sources of cosmetic, medicinal and food ingredients. The selection of the right extraction method and the appropriate type of solvent is very decisive in the acquisition of the target chemical components. The brand of this research focuses on the comparison of extraction between soxhletation and maceration methods in identifying the chemical components of Ketapang leaves (Terminalia Catappa). Sample preparation was carried out by selecting fresh, cleaned, dried and mashed Ketapang leaves. The extraction was carried out in two stages using two types of solvents, namely the first stage of extraction using ethanol. Obtained a dilute extract, then concentrated using a rotary evaporator. The second extraction used n-hexane as solvent. There are 4 kinds of extracts, each ethanol extract and n-hexane extract by applying the soxhletation and maceration method. The results obtained showed that: the application of the maceration method to the identification of chemical components of ketapang leaves gave relatively better separation results than the soxhletation method. The number of chemical components identified from the ethanol extract of ketapang leaves is ± 20 species which are dominated by fatty acid compounds. There are two groups of chemical compounds identified from ketapang leaves using n-hexane as solvent both in the application of soxhletation and maceration methods with high similarity 90%, namely 4 kinds of chemical components of the fatty acid group (tetradecanoic acid, Hexadecanoic, Octadecanoid, Octadeca-9,12 -Dienoite) and 2 kinds of aliphatic components (methyl cyclopentane, Tetraco Hexane)

Downloads

Download data is not yet available.

Author Biographies

Ismail Marzuki, Fajar University

Chemical Engineering

Melisa Mirsyah, Universitas Fajar

Mahasiswa Tugas Akhir Strata 1 Teknik Kimia UNIFA

Selfina Gala, Universitas Fajar

Dosen Prodi Teknik Kimia sebagai Pembimbing 2 Mahasiswa

References

Agustini, N., & Wayan S. 2017. Identifikasi Senyawa Aktif dan Toksisitas Hayati Ekstrak n-heksana, Etil Asetat dan etanol Mikroalga Tetraselmis chuii Secara Brine Shrimp Lethality Test (BSLT). Warta Industri Hasil Pertanian, 34(1), 8–17. https://doi.org/10.32765/wartaihp.v34i1.4063

Amelinda, E., Widarta, I. W. R., & Darmayanti, L. P. T. 2018. Pengaruh Waktu Maserasi terhadap Aktivitas Antioksidan Ekstrak Rimpang Temulawak (Curcuma xanthorriza Roxb.). Jurnal Ilmu Dan Teknologi Pangan (ITEPA), 7(4), 165–174. https://doi.org/10.24843/itepa.2018. v07.i04.p03

Asbanu, Y. W. A., Wijayati, N., & Kusumo, E. (2019). Identifikasi Senyawa Kimia Ekstrak Daun Sirsak (Annona muricata L.) dan Uji Aktivitas Antioksidannya dengan Metode DPPH (2,2-Difenil-1- Pikrilhidrasil). Indonesian Journal of Chemical Science, 8(3), 153–160.

Aslamiah, S., & Haryadi. 2014. Identifikasi Kandungan Kimia Golongan Senyawa Daun Pohon Kapuk (Ceiba pentandra L.) sebagai Obat Tradisional. Anterior Jurnal, 14(1), 11–19.

Chairunnisa, S., Wartini, N. M., & Suhendra, L. 2019. Pengaruh Suhu dan Waktu Maserasi terhadap Karakteristik Ekstrak Daun Bidara (Ziziphus mauritiana L.) sebagai Sumber Saponin. Jurnal Rekayasa Dan Manajemen Agroindustri, 7(4), 551–560. https://doi.org/10.24843/jrma.2019. v07.i04.p07

Encik Eko Rifkowaty, & Wardanu, A. P. 2016. Pengaruh Ekstraksi Cara Basah Dan Cara Kering Terhadap Aktivitas Antioksidan Ekstrak Cengkodok (Melastoma Malabathricum L.). Jurnal Aplikasi Teknologi Pangan, 5(1), 10–15. https://doi.org/10.17728/jatp.v5i1.33

Hanif, R. M. A., Kartika, R., & Simanjuntak, P. 2016. Isolation and Identification of Chemical Compound from n -Hexane Extract of Orange Stem Parasite (Dendrophtoe pentandra ( L .). Jurnal Kimia Mulawarman, 14(1), 36–41.

Hasnidar, Tasmin, Sitorus, S., Hidayati, W., Mustar, Fhirawati, … Sulfianti. 2020. Ilmu Kesehatan Masyarakat. (A. Rikki, Ed.). Medan: Yayasan Kita Menulis.

Kamaruddin, M., Ma’ruf, N., Ningsih, S., & Marzuki, I. 2017. Pemanfaatan Limbah Biji Durian sebagai Bahan Dasar Donat Bergizi Tinggi Berdasarkan Uji Organoleptik. In Seminar Nasional Inovasi Teknologi Hasil Perkebunan (pp. 225–231).

Kamaruddin, M., Marzuki, I., Burhan, A., & Ahmad, R. 2021. Screening acetylcholinesterase inhibitors from marine-derived actinomycetes by simple chromatography. In The 1st International Conference on Biotechnology and Food Sciences IOP Conf. Series: Earth and Environmental Science (Vol. 679, p. 012011). https://doi.org/10.1088/1755-1315/679/1/012011

Marzuki, I. (2021). Pengantar Kimia Organik Fisis. (A. Noor, Ed.) (1st ed.). Makassar: Tohar Media.

Marzuki, I., & Erniati. 2017. Skrining Spons Potensial Sebagai Biodegradator Hidrokarbon Berdasarkan Data Morfologi. Prosiding Seminar Nasional Hasil Penelitian (SNP2M), 1(1), 43–48. https://doi.org/10.17605/OSF.IO/G3ZYA

Marzuki, I., Gusty, S., Armus, R., Sapar, A., Asaf, R., Athirah, A., & Jaya. 2021. Secondary Metabolite Analysis and Anti-Bacteria and Fungal Activities of Marine Sponge Methanol Extract Based on Coral Cover. In The 6th International Conference on Basic Sciences (IAP Conf. Proc.) (Vol. 2360, pp. 1–9). https://doi.org/10.1063/5.0059500

Marzuki, I., Vinolina, N. S., Harahap, R., Arsi, Ramdan, E. P., Simarmata, M. M., … Ilhami, W. T. 2021. Budi Daya Tanaman Sehat Secara Organik. (R. Watrianthos, Ed.). Medan, Yayasan Kita Menulis

Maulida, C., Kusrini, D., & Fachriyah, E. 2012. Isolasi, Identifikasi serta Uji Aktivitas Sitotoksik Senyawa Alkaloid Total Daun Ketapang (Terminalia Catappa Linn.) dengan Metode Brine Shrimp Lethality Test (BSLT). Jurnal Kimia Sains Dan Aplikasi, 15(1), 13–17. https://doi.org/10.14710/jksa.15.1.13-17

Pandiangan, E., Edison, & Ilza, M. 2020. Pengaruh Penggunaan Pelarut Organik yang Berbeda terhadap Sifat Fisika-Kimia Ekstrak Minyak Ikan Tembakul, (Periopthalmodon schlosseri). Endocrine, 9(May), 6. Retrieved from https://www.slideshare.net/maryamkazemi3/stability-of-colloids%0Ahttps://

Pattola, P., Nur, A., Atmadja, T. F. A.-G., Yunianto, A. E., Marzuki, I., Unsunnidhal, L., … Purba, A. M. V. 2020. Gizi, Kesehatan dan Penyakit. (Alex Rikki, Ed.). Medan: Yayasan Kita Menulis. Retrieved from https://kitamenulis.id/2020/11/19/gizi-kesehatan-dan-penyakit/

Purba, B., Nainggolan, L. E., Siregar, R. T., Chaerul, M., Simarmata, M. M., Bachtiar, E., … Meganingratna, A. 2020. Ekonomu Sumber Daya Alam. (J. Simarmata, Ed.). Medan: Yayasan Kita Menulis. Retrieved from https://kitamenulis.id/2020/10/08/ekonomi-sumber-daya-alam-sebuah-konsep-fakta-dan-gagasan/

Purba, D. H., Marzuki, I., Dailami, M., Saputra, H. A., Mawarti, H., Gurning, K., … Purba, A. M. V. 2021. Biokimia. (R. Watrianthos, Ed.). Medan: Yayasan Kita Menulis.

Putra, C. D. P., Fachriyah, E., & Kusrini, D. 2011. Isolasi, Identifikasi dan Uji Toksisitas Senyawa Steroid dalam Ekstrak Kloroform Daun Ketapang (Terminalia catappa Linn). Jurnal Kimia Sains Dan Aplikasi, 14(1), 4–7. https://doi.org/10.14710/jksa.14.1.4-7

Rahmadani, N., Ruslan, R., & Satrimafitrah, P. 2018. Penerapan Metode Ekstrak Pelarut dalam Pemisahan Minyak Atsiri Jahe Merah (Zingiber officinale Var.Rubrum). KOVALEN: Jurnal Riset Kimia, 4(1), 74–81. https://doi.org/10.22487/kovalen.2018.v4.i1.10186

Riskitavani, D. V., & Purwati, K. I. 2013. Studi Potensi Bioherbisida Ekstrak Daun Ketapang (Terminalia catappa) terhadap Gulma Rumput Teki (Cyperus rotundus). Sains Dan Seni Pomits, 2(2), 59–63.

Simarmata, M. M., Sudarmanto, E., Kato, I., Nainggolan, L. E., Purba, E., Sutrisno, E., … Mastutie, F. 2021. Ekonomi Sumber Daya Alam. (A. Karim, Ed.), Yayasan Kita Menuli. Medan: Yayasan Kita Menulis.

Suryowati, T., Damanik, R., Bintang, M., & Handharyani, E. 2015. Identifikasi Komponen Kimia Dan Aktivitas Antioksidan Dalam Tanaman Torbangun (Coleus Amboinicus Lour). Jurnal Gizi Pangan, 10(3), 217–224. https://doi.org/10.25182/jgp.2015.10.3.

Tampemawa, P. V, Pelealu, J. J., & Kandou, F. E. F. 2016. Uji Efektivitas Ekstrak Daun Ketapang (Terminalia Catappa L.) Terhadap Bakteri Bacillus Amyloliquefaciens. Pharmacon, 5(1), 308–320. https://doi.org/10.35799/pha.5.2016.11324

Utami, N. F., Nurdayanty, S. M., & Sutanto, U. S. 2020. Pengaruh Berbagai Metode Ekstraksi pada Penentuan Kadar Flavanoid Ekstrak Etanol Daun Iler (Plectranthus scutellarioides). FITOFARMAKA: Jurnal Ilmiah Farmasi, 10(1), 76–83. https://doi.org/10.33751/jf.v10i1.2069

Wijaya, D. R., Paramitha, M., & Putri, N. P. 2019. Ekstraksi Oleoresin Jahe Gajah (Zingiber officinale var. officinarum) dengan Metode Sokletasi. Jurnal Konversi, 8(1), 9–16.

Published
2022-06-25
How to Cite
Marzuki, I., Mirsyah, M., & Gala, S. (2022). Identifikasi Komponen Kimia Ekstrak Daun Ketapang (Terminalia cattapa) Berdasarkan Perbandingan Metode Ekstraksi. Al-Kimia, 10(1). https://doi.org/10.24252/al-kimia.v10i1.25457
Section
Article
Abstract viewed = 2343 times