Sintesis dan Karakterisasi Hidroksiapatit Dari Tulang Ikan Tuna (Thunnus Albacores) Dengan Xrf, Ftir, Dan Xrd
Abstract
Hydroxyapatite (Hap) were inorganic compounds with constituent of bones and teeth has the molecular formula Ca5(PO4)3OH. Synthesis of hydroxyapatite can be done with hydrothermal method with calcium precursors tuna fish bone calcination process to obtain calcium compounds in the form of calcium oxide. Calsium wich has been obtained added phosphate precursor NH4H2PO4 0.547 M. On research conducted long stirring time variation and its effect on rendement and the resulting crystallites products. As for the variation of the long time of stirring used are 1, 2, 3, 4 and 5 hours. The optimum time of formation of hydroxyapatite obtained within 3 hours stirring from which content was 96.4156%. The material was analyzed by FTIR,XRF and XRD. Results showed their characterization by FTIR indicated the presence of OH groups,PO4 and CO3. Based on the resulting diffraction of XRF and XRD analysis, crystallite size obtained each of 41,9753 within 2 hours of stirring structure was hexagonal.
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References
Aisyah & Dara. (2012). Program Pemanfaatan Sisa Tulang Ikan Untuk Produk Hidroksiapatit: Kajian Di Pabrik Pngolahan Kerupuk Lekor Kuala Trengganu-Malaysia. Jurnal Sosioteknologi Edisi 26 : 129-141.
Alqap, Sofwan Faturohman dan Iis Sopyan. (2009). Low Temperature Hydrothermal Synthesis of Calcium Phosphate Ceramics: Effect of excess Ca precursor on phase behavior. Indian Journal of Chemistry , 4 (A): 142-150.
Amri, Said & Khairuman Suminar. (2008) .Jendela IPTEK. Jakarta: PT
Balai Pustaka. Fitriawan & Margi. (2014). Sintesis Hidroksiapatit Berbahan Dasar Tulang Sapi Dengan Metode Pretipitasi Sebagai Kandidat Pengganti Graft. Prosiding SNMF : 1-5.
Hui. P. (2010) Synthesis of Hydroxyapatite Bio-Ceramic Powder by Hydrothermal Method. Journal of minerals and materials characterization & engineering, 9 (8) : 683-692.
Nabil, M. (2005). Pemanfaatan Limbah Tulang Ikan tuna (Thunus sp.) Sebagai Sumber Kalsium Dengan Metode Hidrolisis Protein. [Skripsi]. Fakultas Perikanan dan Ilmu Kelautan, Institut Pertanian Bogor.
Nayak & Amit Kumar. (2010). Hydroxyapatite Synthesis Methodologies: An Overview. International Journal Of Chemtech Reasearch, 2(2) : 903-907.
Nurilmala, M., Wahyuni, M., & Wiratmaja, H. (2006). Perbaikan Nilai Tambah Limbah Tulang Ikan Tuna (Thunnus Sp) Menjadi Gelatin Serta AnalisisFisika-Kimia. Buletin Teknologi Hasil Perikanan. Alumni Program Studi Teknologi Hasil Perikanan, FPIK, IPB. 9(2):22-33.
Suchanek, Wojciech, L & Richard, E. (2006) Hydrothermal Synthesisf Advanced Ceramic Powders. Advances in Science and Technology, 45 : 184-193.
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