KARAKTERISASI MIKROKRISTALIN SELULOSA DARI KULIT JAGUNG PULUT (Zea mays L. Var Ceratina Kulesh)
Abstract
Corn husk is a part of the plant that has a high cellulose fiber content, which is around 44.08%, so it is potentially to be used as a source of raw material of microcrystalline cellulose. The purpose of this research was to synthesize and determine the characteristics of microcrystalline cellulose produced from corn husk. The making of microcrystalline cellulose was carried out in two stages, namely delignification using NaOH solvent with five variations of concentration (7,5%, 10%, 12,5%, 15% and 17,5%) and hydrolyzed using 2,5 N HCl. Characteristic test for microcrystalline cellulose included organoleptic, pH, flow time and stationary angle, FTIR, and XRD. The results showed that microcrystalline cellulose produced from corn husk had characteristics such as fine powder, white and odorless, pH was 7.0, flow time was 0.3 g/sec, a stationary angle was 54o, FTIR analysis showed a typical peak of cellulose namely 3411,05 for O-H and 2900,61 for C-H, with a crystallinity degree was 79%.Downloads
References
Coniwanti, P. (2015). Pembuatan Natrium Karboksimetil Selulosa (Na-CMC) dari Selulosa Limbah Kulit Kacang (Arachis hypogea L.). Jurnal Teknik Kimia, 21(4), 57–64.
Faesal, F. (2013). Pengolahan limbah tanaman jagung untuk pakan ternak sapi potong. Seminar Nasional Inovasi Teknologi Pertanian, 19, 181–190.
Fagbemigun, T. K., Fagbemi, O. D., Otitoju, O., Mgbachiuzor, E., & Igwe, C. C. (2014). Pulp and paper-making potential of corn husk. International Journal of AgriScience, 4(44), 209–213.
Hening Pratiwi, L. I. A. Y. L. M. (2015). Uji Karakteristik Mikrokristalin Selulosa dari Nata De Soya sebagai Eksipien Tablet. Farmasains, 2(6), 269–274.
Kharismi, R. R. A. Y., Sutriyo, & Suryadi, H. (2018). Preparation and characterization of microcrystalline cellulose produced from betung bamboo (dendrocalamus asper) through acid hydrolysis. Journal of Young Pharmacists, 10(2), s79–s83. https://doi.org/10.5530/jyp.2018.2s.15
Maruapey, A. (2012). Produksi Produksi Berbagai Jagung Pulut. Jurnal Ilmiah Agribisnis Dan Perikanan, 5(2), 33–45.
Prasetia Jemmy A., I., Dewantara Putra, , Permata Sari Arsana, D., & Merlina Prabayanti, N. (2016). Studi Karakteristik Farmasetis Mikrokristalin Selulosa dari Jerami Padi Varietas Lokal Bali. Indonesian Journal of Materials Science, 17(3).
Raymond C. Rowe, et al. (2012). Handbook of Pharmaceutical Excipients (7th ed.). Pharmaceutical Press.
RI, D. K. dan A. K. (2017). Fasilitasi Pengembangan dan Peningkatan Kapasitas Produksi Bahan Baku Obat dan Bahan Baku Obat Tradisional. 12.
Statistik, B. P. (2020). No Title. https://www.bps.go.id/linkTableDinamis/view/id/868
Steven, . M., & Suratman, R. (2014). PEMBUATAN MIKROKRISTALIN SELULOSA ROTAN MANAU (Calamus manan sp.) SERTA KARAKTERISASINYA. Jurnal Selulosa, 4(02), 89–96. https://doi.org/10.25269/jsel.v4i02.84
Suarni, S., Aqil, M., & Subagio, H. (2019). POTENSI PENGEMBANGAN JAGUNG PULUT MENDUKUNG DIVERSIFIKASI PANGAN / Potency of Waxy Corn Development to Support Food Diversification. Jurnal Penelitian Dan Pengembangan Pertanian, 38(1), 1. https://doi.org/10.21082/jp3.v38n1.2019.p1-12
Sumada, K., Erka Tamara, P., & Alqani, F. (2011). Kajian Proses Isolasi Α -Selulosa Dari Limbah Batang Tanaman Manihot Esculenta Crantz Yang Efisien. Jurnal Teknik Kimia, 5(2), 434–438.
Sumaiyah, Wirjosentono, B., & Karsono. (2016). Utilization of microcrystalline cellulose of sugar palm bunches (Arengapinnata (wurmb) merr.)asexcipients tablet direct compression. International Journal of PharmTech Research, 9(7), 130–139.
Trache, D., Hussin, M. H., Hui Chuin, C. T., Sabar, S., Fazita, M. R. N., Taiwo, O. F. A., Hassan, T. M., & Haafiz, M. K. M. (2016). Microcrystalline cellulose: Isolation, characterization and bio-composites application—A review. International Journal of Biological Macromolecules, 93, 789–804. https://doi.org/10.1016/j.ijbiomac.2016.09.056
Uwaezuoke, O. J., Bamiro, O. A., Ngwuluka, N. C., Ajalla, O. T., & Okinbaloye, A. O. (2014). Comparative evaluation of the disintegrant properties of rice husk cellulose, corn starch and Avicel® in metronidazole tablet formulation. Journal of Applied Pharmaceutical Science, 4(12), 112–117. https://doi.org/10.7324/JAPS.2014.41219
Widia, I., & Wathoni, N. (2014). Review artikel selulosa mikrokristal: isolasi, karakterisasi dan aplikasi dalam bidang farmasetik. Jurnal Farmaka, 15(2), 127–143.
Z Hindi, S. S. (2017). Microcrystalline Cellulose: The Inexhaustible Treasure for Pharmaceutical Industry. Nanoscience and Nanotechnology Research, 4(1), 17–24. https://doi.org/10.12691/nnr-4-1-3
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